Material Science Research Papers/Topics

Open-source Parametric 3-D Printed Slot Die System for Thin Film Semiconductor Processing

Slot die coating is growing in popularity because it is a low operational cost and easily scaled processing technique for depositing thin and uniform films rapidly, while minimizing material waste. The complex inner geometry of conventional slot dies require expensive machining that limits accessibility and experimentation. In order to overcome these issues this study follows an open hardware approach, which uses an open source 3-D printer to both fabricate the slot die and then to functional...

Development of a Resilient 3-D Printer for Humanitarian Crisis Response

Rapid manufacturing using 3-D printing is a potential solution to some of the most pressing issues for humanitarian logistics. In this paper, findings are reported from a study that involved development of a new type of 3-D printer. In particular, a novel 3-D printer that is designed specifically for reliable rapid manufacturing at the sites of humanitarian crises. First, required capabilities are developed with design elements of a humanitarian 3-D printer, which include, (1) fused filament ...

Micromorphology analysis of sputtered indium tin oxide fabricated with variable ambient combinations

Micromorphology analysis of sputtered indium tin oxide fabricated with variable ambient combinations. Abstract This study experimentally investigates the fractal nature of the 3-D surface morphology of sputtered indium tin oxide (ITO) fabricated with five sets of ambient combinations. The samples were prepared on glass substrates by DC magnetron sputtering using argon, argon with oxygen, argon with oxygen and nitrogen, argon with oxygen and hydrogen and argon with oxygen, nitrogen and hydroge...

Effects of silver catalyst concentration in metal assisted chemical etching of silicon

A systematic investigation is performed to determine the effects of the concentration of silver on metal assisted chemical etching (MaCE) on nanostructure formation mechanisms on silicon as well as their resultant optical properties. Silver nitrate concentrations of 0.008M, 0.004M, 0.003M and 0.002M with hydrogen fluoride were used for the preparation of p-type silicon nanostructures. Experimentally it is observed that when the catalysis molarity concentration is decreased in the etching proc...

Properties of Al-Doped Zinc Oxide and In-Doped Zinc Oxide Bilayer Transparent Conducting Oxides towards Solar Cell Applications

Novel aluminum and indium doped zinc oxide bilayer transparent conducting oxide thin films have been developed by simple sol gel spin coating and annealed at 500 C for an hour under nitrogen ambient towards solar cell applications. The structural, electrical and optical properties of both the as deposited and annealed bilayer thin films are characterized. X-ray diffraction studies showed a hexagonal wurtzite-type structure of ZnO with (002) orientation, which was enhanced with annealing. In a...

Design Optimization of Polymer Heat Exchanger for Automated Household-Scale Solar Water Pasteurizer

A promising approach to reducing the >870,000 deaths/year globally from unsafe water is flow-through solar water pasteurization systems (SWPs). Unfortunately, demonstrated systems have high capital costs, which limits access for the poor. The most expensive component of such systems is the heat exchanger (HX). Thus, this study focuses on cost optimization of HX designs for flow-through SWPs using high-effectiveness polymer microchannel HXs. The theoretical foundation for the cost optimization...

Expanding the Consumer Bill of Rights for Material Ingredients

In President John F. Kennedy’s original Consumer Bill of Rights speech to the United States Congress he called for the “right to be informed”. At the time, materials science was in its infancy and only crude information technology was available, so the need for consumers to know what materials their products were made up of was outweighed by the difficulty of providing the information. Fifty-five years later the basic material ingredients are largely unknown for the vast majority of con...

Anisotropic Mechanical Property Variance Between ASTM D638-14 Type I and Type IV Fused Filament Fabricated Specimens

The open source introduction of fused filament fabrication (FFF) enables distributed manufacturing of consumer products. However, with a wide range of low-cost FFF 3-D printers and settings possible, there is a lack of information on the variability in printed mechanical properties. This paper utilizes a large pool of 47 user-assembled 3-D printers to quantify the mechanical property variations of ultimate tensile strength (UTS) and yield strength of FFF printed components using ASTM D638-14 ...

Optimal Design of Thin-film Plasmonic Solar Cells using Differential Evolution Optimization Algorithms

An approach using a differential evolution (DE) optimization algorithm is proposed to optimize design parameters for improving the optical absorption efficiency of plasmonic solar cells (PSC). This approach is based on formulating the parameters extraction as a search and optimization process in order to maximize the optical absorption in the PSC. Determining the physical parameters of three-dimensional (3-D) PSC is critical for designing and estimating their performance, however, due to the ...

Self-sufficiency of 3-D printers: utilizing stand-alone solar photovoltaic power systems

A self-replicating rapid prototyper (RepRap) is a type of 3-D printer capable of printing many of its own components in addition to a wide assortment of products from high-value scientific or medical tools to household products and toys. There is some evidence that these printers could provide low-cost distributed manufacturing in underprivileged rural areas. For the most isolated communities without access to the electric grid, a low-cost alternative energy is needed. Solar energy can be har...

Expanded microchannel heat exchanger: Non-destructive evaluation

Recent theoretical developments in expanded microchannel polymer-based heat exchangers were promising, but the initial experiments underperformed simple theory. In order to understand this discrepancy, this paper introduces a nondestructive methodology for characterizing polymer heat exchangers. A computerized tomography (X-ray) scan was performed to diagnose the problem. The method was tested on the expanded microchannel polymer heat exchanger to determine the variations in geometry between ...

Chemical Compatibility of Fused Filament Fabrication-based 3-D Printed Components with Solutions Commonly Used in Semiconductor Wet Processing

3-D printing shows great potential in laboratories for making customized labware and reaction vessels. In addition, affordable fused filament fabrication (FFF)-based 3-D printing has successfully produced high-quality and affordable scientific equipment, focusing on tools without strict chemical compatibility limitations. As the additives and colorants used in 3-D printing filaments are proprietary, their compatibility with common chemicals is unknown, which has prevented their widespread use...

Prospects of applying 3-D printing to economics of remote communities: reindeer herder case

Purpose – Isolated communities face a variety of inconveniences including severe remoteness, poor roads, extreme climate conditions, resulting in the lack of security of supply chains and exorbitant prices for cargo delivery. The paper investigates the present advantages and prospects of applying 3-D printing to improve economics and everyday life of remote communities, reindeer herder case taken as an example. Design/Methodology/Approach-This study covers the use of a low-cost open-source ...

Fused Particle Fabrication 3-D Printing: Recycled Materials' Optimization and Mechanical Properties

Fused particle fabrication (FPF) (or fused granular fabrication (FGF)) has potential for increasing recycled polymers in 3-D printing. Here, the open source Gigabot X is used to develop a new method to optimize FPF/FGF for recycled materials. Virgin polylactic acid (PLA) pellets and prints were analyzed and were then compared to four recycled polymers including the two most popular printing materials (PLA) and acrylonitrile butadiene styrene (ABS)) as well as the two most common waste plastic...

Economic Advantages of Dry-Etched Black Silicon in Passivated Emitter Rear Cell (PERC) Photovoltaic Manufacturing

Industrial Czochralski silicon (Cz-Si) photovoltaic (PV) efficiencies have routinely reached >20% with the passivated emitter rear cell (PERC) design. Nanostructuring silicon (black-Si) by dry-etching decreases surface reflectance, allows diamond saw wafering, enhances metal gettering, and may prevent power conversion efficiency degradation under light exposure. Black-Si allows a potential for >20% PERC cells using cheaper multicrystalline silicon (mc-Si) materials, although dry-etching is wi...


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